Information card for entry 7704706

Structure parameters

• Formula: C13 H24 Br Ge N3
• Calculated formula: C13 H24 Br Ge N3
• Title of publication: Cooperative N-H bond activation by amido-Ge(ii) cations.
• Authors of publication: Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9495 - 9504
• a: 7.3994 ± 0.0015 Å
• b: 10.027 ± 0.002 Å
• c: 21.82 ± 0.004 Å
• α: 90°
• β: 91.18 ± 0.03°
• γ: 90°
• Cell volume: 1618.6 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0997
• Residual factor for significantly intense reflections: 0.0977
• Weighted residual factors for significantly intense reflections: 0.2646
• Weighted residual factors for all reflections included in the refinement: 0.2661
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No