Information card for entry 7704707

Structure parameters

• Formula: C31 H33 Cl Ge N P
• Calculated formula: C31 H33 Cl Ge N P
• SMILES: [Ge]1(Cl)[P](c2c(CN1c1c(cccc1C(C)C)C(C)C)cccc2)(c1ccccc1)c1ccccc1
• Title of publication: Cooperative N-H bond activation by amido-Ge(ii) cations.
• Authors of publication: Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9495 - 9504
• a: 9.1837 ± 0.0003 Å
• b: 11.0396 ± 0.0004 Å
• c: 14.5439 ± 0.0005 Å
• α: 111.357 ± 0.003°
• β: 92.618 ± 0.003°
• γ: 90.475 ± 0.003°
• Cell volume: 1371.34 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0275
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for significantly intense reflections: 0.0653
• Weighted residual factors for all reflections included in the refinement: 0.0672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No