Information card for entry 7704708

Structure parameters

• Formula: C18 H26 Br Ge N3
• Calculated formula: C18 H26 Br Ge N3
• SMILES: Br[Ge]1N(C(C)(C)C)CCN2C=1N(C=C2)c1c(cc(cc1C)C)C
• Title of publication: Cooperative N-H bond activation by amido-Ge(ii) cations.
• Authors of publication: Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9495 - 9504
• a: 13.8454 ± 0.0003 Å
• b: 13.2083 ± 0.0003 Å
• c: 21.4808 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3928.28 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.0983
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No