Information card for entry 7704828

Structure parameters

• Formula: C22 H36 Cl Ge N3 Si
• Calculated formula: C22 H36 Cl Ge N3 Si
• Title of publication: An unsaturated amido-substituted six-vertex germanium cluster and its reactions with alkenes and alkynes.
• Authors of publication: Helmer, Joschua; Hepp, Alexander; Lips, Felicitas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 34
• Pages of publication: 11843 - 11850
• a: 9.9016 ± 0.0002 Å
• b: 13.3519 ± 0.0003 Å
• c: 18.7267 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2475.77 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.023
• Residual factor for significantly intense reflections: 0.022
• Weighted residual factors for significantly intense reflections: 0.0584
• Weighted residual factors for all reflections included in the refinement: 0.0587
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No