Information card for entry 7704829

Structure parameters

• Formula: C60 H104 Ge6 N4 Si4
• Calculated formula: C60 H104 Ge6 N4 Si4
• Title of publication: An unsaturated amido-substituted six-vertex germanium cluster and its reactions with alkenes and alkynes.
• Authors of publication: Helmer, Joschua; Hepp, Alexander; Lips, Felicitas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 34
• Pages of publication: 11843 - 11850
• a: 16.4377 ± 0.0007 Å
• b: 16.4377 ± 0.0007 Å
• c: 27.2437 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7361.2 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0423
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.193
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No