Information card for entry 7705084

Structure parameters

• Formula: C75 H82 O4 S4 Sn
• Calculated formula: C75 H82 O4 S4 Sn
• Title of publication: Synthesis and structures of diaryloxystannylenes and -plumbylenes embedded in 1,3-diethers of thiacalix[4]arene.
• Authors of publication: Kuriki, Ryunosuke; Kuwabara, Takuya; Ishii, Youichi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 35
• Pages of publication: 12234 - 12241
• a: 12.094 ± 0.003 Å
• b: 12.497 ± 0.003 Å
• c: 22.902 ± 0.006 Å
• α: 83.617 ± 0.01°
• β: 85.056 ± 0.011°
• γ: 75.959 ± 0.009°
• Cell volume: 3330.8 ± 1.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1081
• Residual factor for significantly intense reflections: 0.0851
• Weighted residual factors for significantly intense reflections: 0.1655
• Weighted residual factors for all reflections included in the refinement: 0.1827
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No