Information card for entry 7705085

Structure parameters

• Formula: C131 H208 O8 Pb2 S8 Si4
• Calculated formula: C131 H208 O8 Pb2 S8 Si4
• Title of publication: Synthesis and structures of diaryloxystannylenes and -plumbylenes embedded in 1,3-diethers of thiacalix[4]arene.
• Authors of publication: Kuriki, Ryunosuke; Kuwabara, Takuya; Ishii, Youichi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 35
• Pages of publication: 12234 - 12241
• a: 13.4391 ± 0.0008 Å
• b: 13.7334 ± 0.0007 Å
• c: 20.3149 ± 0.001 Å
• α: 71.319 ± 0.003°
• β: 77.604 ± 0.003°
• γ: 77.966 ± 0.003°
• Cell volume: 3429.3 ± 0.3 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0683
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No