Information card for entry 7705086

Structure parameters

• Formula: C58 H86 O4 S4 Si2 Sn
• Calculated formula: C58 H86 O4 S4 Si2 Sn
• Title of publication: Synthesis and structures of diaryloxystannylenes and -plumbylenes embedded in 1,3-diethers of thiacalix[4]arene.
• Authors of publication: Kuriki, Ryunosuke; Kuwabara, Takuya; Ishii, Youichi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 35
• Pages of publication: 12234 - 12241
• a: 13.377 ± 0.0012 Å
• b: 17.7497 ± 0.0015 Å
• c: 25.887 ± 0.002 Å
• α: 90°
• β: 102.696 ± 0.002°
• γ: 90°
• Cell volume: 5996.3 ± 0.9 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0899
• Goodness-of-fit parameter for all reflections included in the refinement: 1.118
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No