Information card for entry 7705483

Structure parameters

• Formula: C36 H41 F12 N5 Os Sb2
• Calculated formula: C36 H41 F12 N5 Os Sb2
• SMILES: [Os]123456([n]7ccccc7C[N]1=C(Nc1ccc(cc1)C)Nc1ccc(cc1)C)([n]1ccccc1)[c]1([cH]6[cH]5[c]4([cH]3[cH]21)C(C)C)C.[Sb](F)(F)(F)(F)([F-])F.[Sb](F)(F)(F)(F)(F)[F-]
• Title of publication: Half-sandwich complexes of osmium containing guanidine-derived ligands.
• Authors of publication: Parker, Amie; Lamata, Pilar; Viguri, Fernando; Rodríguez, Ricardo; López, José A; Lahoz, Fernando J.; García-Orduña, Pilar; Carmona, Daniel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13601 - 13617
• a: 11.5507 ± 0.0013 Å
• b: 11.8469 ± 0.0013 Å
• c: 15.5684 ± 0.0017 Å
• α: 72.569 ± 0.001°
• β: 80.229 ± 0.001°
• γ: 82.14 ± 0.002°
• Cell volume: 1994.7 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.106
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1153
• Weighted residual factors for all reflections included in the refinement: 0.1352
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No