Information card for entry 7705484

Structure parameters

• Formula: C40 H45 Cl2 F6 N3 Os P Sb
• Calculated formula: C39 H43 F6 N3 Os P Sb
• SMILES: [Os]1234567([P](c8ccccc8)(c8ccccc8)CC[N]1=C(N2c1ccc(cc1)C)Nc1ccc(cc1)C)[c]1([cH]3[cH]4[c]5([cH]6[cH]71)C(C)C)C.[Sb](F)(F)(F)([F-])(F)F
• Title of publication: Half-sandwich complexes of osmium containing guanidine-derived ligands.
• Authors of publication: Parker, Amie; Lamata, Pilar; Viguri, Fernando; Rodríguez, Ricardo; López, José A; Lahoz, Fernando J.; García-Orduña, Pilar; Carmona, Daniel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13601 - 13617
• a: 24.6016 ± 0.0011 Å
• b: 10.2764 ± 0.0005 Å
• c: 16.4397 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4156.2 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0257
• Residual factor for significantly intense reflections: 0.0232
• Weighted residual factors for significantly intense reflections: 0.0557
• Weighted residual factors for all reflections included in the refinement: 0.0572
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No