Information card for entry 7705891

Structure parameters

• Formula: Dy3 K5 Na5.34 Ni O139.78 Sb3 W30
• Calculated formula: Dy3 K5 Na5.3333 Ni O139.773 Sb3 W30
• Title of publication: Ionic strength effect on regulating the synthetic assembly of polyoxometalate clusters with slow magnetic relaxation behavior.
• Authors of publication: Cai, Jing; Ye, Run; Liu, Xinhao; Guo, Leilei; Qiao, Xinrong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 46
• Pages of publication: 16954 - 16961
• a: 18.2445 ± 0.0006 Å
• b: 19.9956 ± 0.0007 Å
• c: 24.4742 ± 0.0006 Å
• α: 93.078 ± 0.002°
• β: 99.426 ± 0.002°
• γ: 116.645 ± 0.003°
• Cell volume: 7790.2 ± 0.5 ų
• Cell temperature: 186 ± 2 K
• Ambient diffraction temperature: 186 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1293
• Residual factor for significantly intense reflections: 0.0832
• Weighted residual factors for significantly intense reflections: 0.1928
• Weighted residual factors for all reflections included in the refinement: 0.2263
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No