Information card for entry 7705892

Structure parameters

• Formula: Ni0.21 O9.26 Sb0.21 W2.11
• Calculated formula: Ni0.210526 O9.26316 Sb0.210526 W2.10526
• Title of publication: Ionic strength effect on regulating the synthetic assembly of polyoxometalate clusters with slow magnetic relaxation behavior.
• Authors of publication: Cai, Jing; Ye, Run; Liu, Xinhao; Guo, Leilei; Qiao, Xinrong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 46
• Pages of publication: 16954 - 16961
• a: 17.8033 ± 0.0014 Å
• b: 18.5672 ± 0.0016 Å
• c: 14.166 ± 0.0012 Å
• α: 90°
• β: 113.239 ± 0.009°
• γ: 90°
• Cell volume: 4302.8 ± 0.7 ų
• Cell temperature: 178.3 ± 0.6 K
• Ambient diffraction temperature: 178.3 ± 0.6 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0814
• Residual factor for significantly intense reflections: 0.0678
• Weighted residual factors for significantly intense reflections: 0.1689
• Weighted residual factors for all reflections included in the refinement: 0.1788
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No