Information card for entry 7705893

Structure parameters

• Formula: Dy3 K4 Na4.75 O138.33 Sb3 W31
• Calculated formula: Dy3 K4 Na4.75 O138.333 Sb4 W30
• Title of publication: Ionic strength effect on regulating the synthetic assembly of polyoxometalate clusters with slow magnetic relaxation behavior.
• Authors of publication: Cai, Jing; Ye, Run; Liu, Xinhao; Guo, Leilei; Qiao, Xinrong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 46
• Pages of publication: 16954 - 16961
• a: 35.159 ± 0.003 Å
• b: 18.5597 ± 0.0007 Å
• c: 48.357 ± 0.003 Å
• α: 90°
• β: 114.193 ± 0.009°
• γ: 90°
• Cell volume: 28783 ± 4 ų
• Cell temperature: 191 ± 2 K
• Ambient diffraction temperature: 191 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1583
• Residual factor for significantly intense reflections: 0.1059
• Weighted residual factors for significantly intense reflections: 0.2022
• Weighted residual factors for all reflections included in the refinement: 0.2298
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No