Information card for entry 7705987

Structure parameters

• Formula: C68 H120 Li2 N4 O2 P4 Rh2 Si8
• Calculated formula: C68 H120 Li2 N4 O2 P4 Rh2 Si8
• Title of publication: Forays into rhodium macrocyclic chemistry stabilized by a P₂N₂ donor set. Activation of dihydrogen and benzene.
• Authors of publication: Yeo, Alyssa; Sanz, Corey A.; Fryzuk, Michael D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 3
• Pages of publication: 899 - 907
• a: 10.7614 ± 0.0005 Å
• b: 22.3119 ± 0.0013 Å
• c: 17.1063 ± 0.0008 Å
• α: 90°
• β: 92.872 ± 0.002°
• γ: 90°
• Cell volume: 4102.2 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0744
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1307
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No