Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7706852
Preview
Coordinates | 7706852.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Rh(acac)CO(9-phosphatriptycene) complex |
---|---|
Chemical name | (acetylacetonato)-carbonylrhodium-9-phosphatriptycene complex |
Formula | C25 H20 O3 P Rh |
Calculated formula | C25 H20 O3 P Rh |
Title of publication | Sterically hindered ortho-substituted phosphatriptycenes as configurationally stable P-chirogenic triarylphosphines. |
Authors of publication | Hu, Lei; Mahaut, Damien; Tumanov, Nikolay; Wouters, Johan; Collard, Laurent; Robiette, Raphaël; Berionni, Guillaume |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 14 |
Pages of publication | 4772 - 4777 |
a | 9.394 ± 0.0002 Å |
b | 15.7924 ± 0.0003 Å |
c | 16.7012 ± 0.0004 Å |
α | 65.676 ± 0.002° |
β | 80.915 ± 0.002° |
γ | 76.193 ± 0.002° |
Cell volume | 2187.53 ± 0.09 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0262 |
Residual factor for significantly intense reflections | 0.0244 |
Weighted residual factors for significantly intense reflections | 0.0618 |
Weighted residual factors for all reflections included in the refinement | 0.0632 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7706852.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.