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Information card for entry 7706853
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Coordinates | 7706853.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Rh(acac)CO(o-CF3-9-phosphatriptycene complex) |
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Chemical name | (acetylacetonato)-carbonylrhodium-ortho-trifluoromethyl-9-phosphatriptycene complex |
Formula | C26 H19 F3 O3 P Rh |
Calculated formula | C26 H19 F3 O3 P Rh |
Title of publication | Sterically hindered ortho-substituted phosphatriptycenes as configurationally stable P-chirogenic triarylphosphines. |
Authors of publication | Hu, Lei; Mahaut, Damien; Tumanov, Nikolay; Wouters, Johan; Collard, Laurent; Robiette, Raphaël; Berionni, Guillaume |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 14 |
Pages of publication | 4772 - 4777 |
a | 8.26668 ± 0.00008 Å |
b | 15.72226 ± 0.00015 Å |
c | 17.6734 ± 0.00019 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2297.03 ± 0.04 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 6 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0281 |
Residual factor for significantly intense reflections | 0.027 |
Weighted residual factors for significantly intense reflections | 0.0673 |
Weighted residual factors for all reflections included in the refinement | 0.0683 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7706853.html
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