Crystallography Open Database

Information card for entry 7706959

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Coordinates	7706959.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C378 H309 Ag26 B3 Cl7 Cu4 F12 P15
Calculated formula	C378 H309 Ag26 B3.004 Cl7 Cu4 F12.016 P15
Title of publication	The [Ag<sub>25</sub>Cu<sub>4</sub>H<sub>8</sub>Br<sub>6</sub>(CCPh)<sub>12</sub>(PPh<sub>3</sub>)<sub>12</sub>]<sup>3+</sup> : Ag<sub>13</sub>H<sub>8</sub> silver hydride core protected by [CuAg<sub>3</sub>(CCPh)<sub>3</sub>(PPh<sub>3</sub>)<sub>3</sub>]<sup>+</sup> motifs.
Authors of publication	Mikami, Kaiyu; Hui, Shen; Kubo, Kazuyuki; Kume, Shoko; Mizuta, Tsutomu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	16
Pages of publication	5659 - 5665
a	26.339 ± 0.004 Å
b	26.339 Å
c	47.891 ± 0.008 Å
α	90°
β	90°
γ	120°
Cell volume	28773 ± 6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	146
Hermann-Mauguin space group symbol	R 3 :H
Hall space group symbol	R 3
Residual factor for all reflections	0.0828
Residual factor for significantly intense reflections	0.0548
Weighted residual factors for significantly intense reflections	0.1308
Weighted residual factors for all reflections included in the refinement	0.1459
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKa
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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