Information card for entry 7707572

Structure parameters

• Formula: C53 H66 Br N3 Pb
• Calculated formula: C53 H66 Br N3 Pb
• Title of publication: Bis(imino)carbazolate lead(II) fluoride and related halides.
• Authors of publication: Chapple, Peter M.; Hamdoun, Ghanem; Roisnel, Thierry; Carpentier, Jean-François; Oulyadi, Hassan; Sarazin, Yann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9021 - 9025
• a: 20.2426 ± 0.0019 Å
• b: 10.3176 ± 0.0012 Å
• c: 23.505 ± 0.003 Å
• α: 90°
• β: 90.646 ± 0.004°
• γ: 90°
• Cell volume: 4908.8 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0666
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.129
• Goodness-of-fit parameter for all reflections included in the refinement: 0.94
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No