Information card for entry 7707573

Structure parameters

• Formula: C52 H76 N4 Pb Si2
• Calculated formula: C52 H76 N4 Pb Si2
• SMILES: [Pb]12(N([Si](C)(C)C)[Si](C)(C)C)n3c4c(C=[N]2c2c(cccc2C(C)C)C(C)C)cc(cc4c2cc(cc(C=[N]1c1c(cccc1C(C)C)C(C)C)c32)C(C)(C)C)C(C)(C)C
• Title of publication: Bis(imino)carbazolate lead(II) fluoride and related halides.
• Authors of publication: Chapple, Peter M.; Hamdoun, Ghanem; Roisnel, Thierry; Carpentier, Jean-François; Oulyadi, Hassan; Sarazin, Yann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9021 - 9025
• a: 12.9223 ± 0.0007 Å
• b: 13.4651 ± 0.0007 Å
• c: 16.5207 ± 0.001 Å
• α: 69.747 ± 0.002°
• β: 78.014 ± 0.002°
• γ: 76.292 ± 0.002°
• Cell volume: 2595 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0292
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0485
• Weighted residual factors for all reflections included in the refinement: 0.0507
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No