Information card for entry 7707955

Structure parameters

• Common name: Pr(Ph-PDB)3(THF)3
• Chemical name: Nd(BH3Ph2BH3)3(THF)3
• Formula: C48 H72 B6 Nd O3 P3
• Calculated formula: C48 H72 B6 Nd O3 P3
• Title of publication: Mechanochemical synthesis and structural analysis of trivalent lanthanide and uranium diphenylphosphinodiboranates.
• Authors of publication: Fetrow, Taylor V.; Daly, Scott R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 33
• Pages of publication: 11472 - 11484
• a: 11.5469 ± 0.0019 Å
• b: 14.97 ± 0.003 Å
• c: 17.592 ± 0.003 Å
• α: 97.233 ± 0.005°
• β: 96.868 ± 0.005°
• γ: 111.125 ± 0.005°
• Cell volume: 2768.9 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1038
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for significantly intense reflections: 0.1452
• Weighted residual factors for all reflections included in the refinement: 0.1634
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No