Information card for entry 7707956

Structure parameters

• Common name: U(H-PDB)
• Chemical name: U(BH3Ph2BH3)I2(THF)3
• Formula: C12 H24 B2 I2 O3 P U
• Calculated formula: C12 H24 B2 I2 O3 P U
• Title of publication: Mechanochemical synthesis and structural analysis of trivalent lanthanide and uranium diphenylphosphinodiboranates.
• Authors of publication: Fetrow, Taylor V.; Daly, Scott R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 33
• Pages of publication: 11472 - 11484
• a: 9.5213 ± 0.0011 Å
• b: 15.3494 ± 0.0017 Å
• c: 15.8099 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2310.6 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 7
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0771
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for significantly intense reflections: 0.1563
• Weighted residual factors for all reflections included in the refinement: 0.1727
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No