Information card for entry 7708311

Structure parameters

• Formula: C24 H54 As Cl P8
• Calculated formula: C24 H54 As Cl P8
• Title of publication: Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes
• Authors of publication: Eilrich, Volker Jens; Grell, Toni; Lönnecke, Peter; Hey-Hawkins, Evamarie
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 9.0335 ± 0.0004 Å
• b: 13.333 ± 0.0004 Å
• c: 16.5876 ± 0.0006 Å
• α: 68.09 ± 0.003°
• β: 83.488 ± 0.003°
• γ: 81.416 ± 0.003°
• Cell volume: 1829.17 ± 0.12 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.0741
• Weighted residual factors for all reflections included in the refinement: 0.0797
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No