Crystallography Open Database

Information card for entry 7708312

Preview

Coordinates	7708312.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H81 As P12
Calculated formula	C36 H81 As P12
Title of publication	Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes
Authors of publication	Eilrich, Volker Jens; Grell, Toni; Lönnecke, Peter; Hey-Hawkins, Evamarie
Journal of publication	Dalton Transactions
Year of publication	2021
a	13.834 ± 0.0002 Å
b	23.4873 ± 0.0002 Å
c	16.4233 ± 0.0002 Å
α	90°
β	101.098 ± 0.001°
γ	90°
Cell volume	5236.52 ± 0.11 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0577
Residual factor for significantly intense reflections	0.0348
Weighted residual factors for significantly intense reflections	0.0678
Weighted residual factors for all reflections included in the refinement	0.076
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7708312.html