Information card for entry 7708673
| Formula |
C66 H102 Fe2 N4 P6 Si2 |
| Calculated formula |
C66 H102 Fe2 N4 P6 Si2 |
| Title of publication |
Synthesis of Silyl Iron Dinitrogen Complexes for Activation of Dihydrogen and Catalytic Silylation of Dinitrogen |
| Authors of publication |
Chang, Guoliang; Zhang, Peng; Yang, Wenjing; Dong, Yanhong; Xie, Shangqing; Sun, Hongjian; Li, Xiaoyan; Fuhr, Olaf; Fenske, Dieter |
| Journal of publication |
Dalton Transactions |
| Year of publication |
2021 |
| a |
9.9876 ± 0.0003 Å |
| b |
10.4113 ± 0.0003 Å |
| c |
36.5579 ± 0.0006 Å |
| α |
96.856 ± 0.002° |
| β |
91.687 ± 0.002° |
| γ |
116.43 ± 0.002° |
| Cell volume |
3365.15 ± 0.16 Å3 |
| Cell temperature |
172.99 ± 0.1 K |
| Ambient diffraction temperature |
172.99 ± 0.1 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0552 |
| Residual factor for significantly intense reflections |
0.041 |
| Weighted residual factors for significantly intense reflections |
0.0897 |
| Weighted residual factors for all reflections included in the refinement |
0.1003 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.073 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7708673.html
