Crystallography Open Database

Information card for entry 7708729

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Coordinates	7708729.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H112 K2 O12 Si9
Calculated formula	C58 H112 K2 O12 Si9
Title of publication	Silole Allylic Anions Instead of Silanides
Authors of publication	Pöcheim, Alexander; Albers, Lena; Müller, Thomas; Baumgartner, Judith; Marschner, Christoph
Journal of publication	Dalton Transactions
Year of publication	2021
a	11.09 ± 0.004 Å
b	11.339 ± 0.005 Å
c	34.641 ± 0.014 Å
α	88.349 ± 0.006°
β	84.449 ± 0.006°
γ	61.697 ± 0.005°
Cell volume	3817 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.152
Residual factor for significantly intense reflections	0.1444
Weighted residual factors for significantly intense reflections	0.3073
Weighted residual factors for all reflections included in the refinement	0.3114
Goodness-of-fit parameter for all reflections included in the refinement	1.274
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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