Information card for entry 7708730

Structure parameters

• Formula: C45 H93 N Si11
• Calculated formula: C45 H93 N Si11
• Title of publication: Silole Allylic Anions Instead of Silanides
• Authors of publication: Pöcheim, Alexander; Albers, Lena; Müller, Thomas; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 22.157 ± 0.004 Å
• b: 20.831 ± 0.004 Å
• c: 14.438 ± 0.003 Å
• α: 90°
• β: 99.511 ± 0.003°
• γ: 90°
• Cell volume: 6572 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0698
• Weighted residual factors for significantly intense reflections: 0.1432
• Weighted residual factors for all reflections included in the refinement: 0.1463
• Goodness-of-fit parameter for all reflections included in the refinement: 1.26
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No