Information card for entry 7708732

Structure parameters

• Formula: C74 H146 K2 Si20
• Calculated formula: C74 H146 K2 Si20
• Title of publication: Silole Allylic Anions Instead of Silanides
• Authors of publication: Pöcheim, Alexander; Albers, Lena; Müller, Thomas; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 16.821 ± 0.003 Å
• b: 17.503 ± 0.003 Å
• c: 18.76 ± 0.003 Å
• α: 110.608 ± 0.003°
• β: 93.224 ± 0.003°
• γ: 101.578 ± 0.003°
• Cell volume: 5015.9 ± 1.5 ų
• Cell temperature: 496 ± 2 K
• Ambient diffraction temperature: 496.3 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1644
• Residual factor for significantly intense reflections: 0.1429
• Weighted residual factors for significantly intense reflections: 0.2678
• Weighted residual factors for all reflections included in the refinement: 0.2805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No