Information card for entry 7708731

Structure parameters

• Formula: C61 H119 Br Mg O6 Si10
• Calculated formula: C61 H121 Br Mg O6 Si10
• Title of publication: Silole Allylic Anions Instead of Silanides
• Authors of publication: Pöcheim, Alexander; Albers, Lena; Müller, Thomas; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 16.567 ± 0.003 Å
• b: 16.634 ± 0.003 Å
• c: 17.495 ± 0.003 Å
• α: 101.384 ± 0.004°
• β: 98.071 ± 0.004°
• γ: 119.395 ± 0.004°
• Cell volume: 3955.8 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1422
• Residual factor for significantly intense reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.1692
• Weighted residual factors for all reflections included in the refinement: 0.1899
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No