Information card for entry 7708847

Structure parameters

• Formula: C20 H19 Cl O Pb
• Calculated formula: C20 H19 Cl O Pb
• SMILES: [Pb]1([O](C)Cc2c1cccc2)(Cl)(c1ccccc1)c1ccccc1
• Title of publication: Hypercoordinated eka-tin materials with dangling aryl-methoxy and -methylthio ligands exhibiting intramolecular secondary bonding and aryl bond stabilization in reactions with organotin chlorides.
• Authors of publication: Ornelas, Alfredo; Arias-Ugarte, Renzo; Metta-Magaña, Alejandro J; Sharma, Hemant K.; Pannell, Keith H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 44
• Pages of publication: 16084 - 16091
• a: 11.8658 ± 0.0005 Å
• b: 11.9078 ± 0.0005 Å
• c: 12.7241 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1797.86 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0234
• Residual factor for significantly intense reflections: 0.0209
• Weighted residual factors for significantly intense reflections: 0.0396
• Weighted residual factors for all reflections included in the refinement: 0.0401
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No