Information card for entry 7709326

Structure parameters

• Formula: C2 H6 Cl8 Se3 W2
• Calculated formula: C2 H6 Cl8 Se3 W2
• Title of publication: Tungsten(vi) selenide tetrachloride, WSeCl4 – synthesis, properties, coordination complexes and application of [WSeCl4(SenBu2)] for CVD growth of WSe2 thin films
• Authors of publication: Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Sethi, Vikesh; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 6.6025 ± 0.0002 Å
• b: 10.2899 ± 0.0005 Å
• c: 12.2583 ± 0.0006 Å
• α: 89.211 ± 0.004°
• β: 85.388 ± 0.003°
• γ: 81.076 ± 0.003°
• Cell volume: 820.07 ± 0.06 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0459
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0786
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No