Information card for entry 7709329

Structure parameters

• Formula: C28 H26 Cl8 N2 Se2 W2
• Calculated formula: C28 H26 Cl8 N2 Se2 W2
• Title of publication: Tungsten(vi) selenide tetrachloride, WSeCl4 – synthesis, properties, coordination complexes and application of [WSeCl4(SenBu2)] for CVD growth of WSe2 thin films
• Authors of publication: Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Sethi, Vikesh; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 6.03153 ± 0.00011 Å
• b: 15.4384 ± 0.0004 Å
• c: 20.1476 ± 0.0005 Å
• α: 103.815 ± 0.002°
• β: 94.9132 ± 0.0017°
• γ: 98.3755 ± 0.0017°
• Cell volume: 1788.17 ± 0.07 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0503
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.0959
• Weighted residual factors for all reflections included in the refinement: 0.0996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No