Information card for entry 7709328

Structure parameters

• Formula: C4 H12 Cl6 S2 Se3 W2
• Calculated formula: C4 H12 Cl6 S2 Se3 W2
• Title of publication: Tungsten(vi) selenide tetrachloride, WSeCl4 – synthesis, properties, coordination complexes and application of [WSeCl4(SenBu2)] for CVD growth of WSe2 thin films
• Authors of publication: Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Sethi, Vikesh; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 13.5882 ± 0.00013 Å
• b: 19.5279 ± 0.0002 Å
• c: 6.69716 ± 0.00007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1777.08 ± 0.03 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0295
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0705
• Weighted residual factors for all reflections included in the refinement: 0.0706
• Goodness-of-fit parameter for all reflections included in the refinement: 1.188
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No