Information card for entry 7709569

Structure parameters

• Formula: C62 H116 Li4 N4 O2 Si6
• Calculated formula: C62 H116 Li4 N4 O2 Si6
• Title of publication: Trisyl-based multidentate ligands: synthesis and their transition-metal complexes
• Authors of publication: Yin, Zhu-Bao; Wei, Junnian; Xi, Zhenfeng
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 10.0442 ± 0.0003 Å
• b: 16.4938 ± 0.0004 Å
• c: 22.9493 ± 0.0005 Å
• α: 77.906 ± 0.002°
• β: 84.578 ± 0.002°
• γ: 75.704 ± 0.002°
• Cell volume: 3598.77 ± 0.16 ų
• Cell temperature: 180 ± 0.1 K
• Ambient diffraction temperature: 180 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1369
• Weighted residual factors for all reflections included in the refinement: 0.1486
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No