Information card for entry 7709570

Structure parameters

• Formula: C38 H94 Cl2 Mn2 N4 Si6
• Calculated formula: C38 H94 Cl2 Mn2 N4 Si6
• Title of publication: Trisyl-based multidentate ligands: synthesis and their transition-metal complexes
• Authors of publication: Yin, Zhu-Bao; Wei, Junnian; Xi, Zhenfeng
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 9.1109 ± 0.0004 Å
• b: 12.3473 ± 0.0005 Å
• c: 12.7686 ± 0.0006 Å
• α: 101.77 ± 0.004°
• β: 92.549 ± 0.004°
• γ: 99.528 ± 0.003°
• Cell volume: 1382.24 ± 0.11 ų
• Cell temperature: 180 ± 0.1 K
• Ambient diffraction temperature: 180 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for significantly intense reflections: 0.1432
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No