Information card for entry 7709577

Structure parameters

• Formula: C32 H84 Li2 N4 S Si6
• Calculated formula: C32 H84 Li2 N4 S Si6
• Title of publication: Trisyl-based multidentate ligands: synthesis and their transition-metal complexes
• Authors of publication: Yin, Zhu-Bao; Wei, Junnian; Xi, Zhenfeng
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 9.4284 ± 0.0002 Å
• b: 17.4514 ± 0.0004 Å
• c: 29.3718 ± 0.0006 Å
• α: 90°
• β: 92.695 ± 0.002°
• γ: 90°
• Cell volume: 4827.45 ± 0.18 ų
• Cell temperature: 180 ± 0.1 K
• Ambient diffraction temperature: 180 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0922
• Weighted residual factors for all reflections included in the refinement: 0.0961
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No