Crystallography Open Database

Information card for entry 7709578

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Coordinates	7709578.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H71 Cl Mn2 N4 Si6
Calculated formula	C34 H71 Cl Mn2 N4 Si6
Title of publication	Trisyl-based multidentate ligands: synthesis and their transition-metal complexes
Authors of publication	Yin, Zhu-Bao; Wei, Junnian; Xi, Zhenfeng
Journal of publication	Dalton Transactions
Year of publication	2022
a	9.3689 ± 0.0009 Å
b	14.5884 ± 0.0011 Å
c	21.1472 ± 0.0012 Å
α	69.939 ± 0.006°
β	86.262 ± 0.007°
γ	74.947 ± 0.007°
Cell volume	2620.9 ± 0.4 Å³
Cell temperature	180 ± 0.1 K
Ambient diffraction temperature	180 ± 0.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0997
Residual factor for significantly intense reflections	0.0828
Weighted residual factors for significantly intense reflections	0.2128
Weighted residual factors for all reflections included in the refinement	0.2237
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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