Information card for entry 7709940

Structure parameters

• Formula: C24 H60 Al2 N6
• Calculated formula: C24 H60 Al2 N6
• Title of publication: Synthesis and temperature-dependent NMR studies of monomeric and dimeric tris(dialkylamido)alanes
• Authors of publication: Schumann, Erik; Böhme, Uwe; Brendler, Erica; Mertens, Florian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 10.4271 ± 0.0004 Å
• b: 15.5764 ± 0.0006 Å
• c: 19.2818 ± 0.0007 Å
• α: 99.136 ± 0.003°
• β: 91.058 ± 0.003°
• γ: 96.911 ± 0.003°
• Cell volume: 3067.2 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0912
• Weighted residual factors for all reflections included in the refinement: 0.0999
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No