Information card for entry 7709941

Structure parameters

• Formula: C30 H66 Al2 N12
• Calculated formula: C30 H66 Al2 N12
• Title of publication: Synthesis and temperature-dependent NMR studies of monomeric and dimeric tris(dialkylamido)alanes
• Authors of publication: Schumann, Erik; Böhme, Uwe; Brendler, Erica; Mertens, Florian
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 15.3937 ± 0.0005 Å
• b: 15.3937 ± 0.0005 Å
• c: 16.7614 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3971.9 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 4
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0432
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for significantly intense reflections: 0.0889
• Weighted residual factors for all reflections included in the refinement: 0.0963
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No