Information card for entry 7710119

Structure parameters

• Formula: C33 H57 N2 O Si2 Y
• Calculated formula: C33 H57 N2 O Si2 Y
• Title of publication: Sc and Y bis(alkyl) complexes supported by bi- and tridentate amidinate ligands. Synthesis, structure and catalytic activity in polymerization of isoprene and 1-heptene.
• Authors of publication: Trifonov, Alexander; Tolpygin, Aleksei; Sachkova, Anastasia; Mikhailychev, Alexander; Ob’edkov, A. M.; Glukhova, Tatyana; Cherkasov, Anton; Fukin, Georgii K.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.1445 ± 0.0005 Å
• b: 11.4646 ± 0.0005 Å
• c: 15.539 ± 0.0007 Å
• α: 94.646 ± 0.002°
• β: 99.027 ± 0.002°
• γ: 111.26 ± 0.002°
• Cell volume: 1806.72 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0554
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0879
• Weighted residual factors for all reflections included in the refinement: 0.094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No