Information card for entry 7710120

Structure parameters

• Formula: C33 H57 N2 O Sc Si2
• Calculated formula: C33 H57 N2 O Sc Si2
• Title of publication: Sc and Y bis(alkyl) complexes supported by bi- and tridentate amidinate ligands. Synthesis, structure and catalytic activity in polymerization of isoprene and 1-heptene.
• Authors of publication: Trifonov, Alexander; Tolpygin, Aleksei; Sachkova, Anastasia; Mikhailychev, Alexander; Ob’edkov, A. M.; Glukhova, Tatyana; Cherkasov, Anton; Fukin, Georgii K.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.1928 ± 0.0005 Å
• b: 11.3356 ± 0.0005 Å
• c: 15.4964 ± 0.0004 Å
• α: 94.893 ± 0.003°
• β: 98.012 ± 0.003°
• γ: 111.928 ± 0.004°
• Cell volume: 1785.79 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0564
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.1161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No