Information card for entry 7710513

Structure parameters

• Formula: C31 H51 F3 Ge N2 O3 S Si2
• Calculated formula: C31 H51 F3 Ge N2 O3 S Si2
• Title of publication: Covalent triflates as synthons for silolyl- and germolyl cations
• Authors of publication: Wohltmann, Wiebke Marie; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.5742 ± 0.0004 Å
• b: 18.7345 ± 0.0006 Å
• c: 30.6586 ± 0.001 Å
• α: 90°
• β: 93.066 ± 0.002°
• γ: 90°
• Cell volume: 7211.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0581
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections included in the refinement: 0.1064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No