Information card for entry 7710514

Structure parameters

• Formula: C29 H33 F3 O3 S Si3
• Calculated formula: C29 H33 F3 O3 S Si3
• Title of publication: Covalent triflates as synthons for silolyl- and germolyl cations
• Authors of publication: Wohltmann, Wiebke Marie; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 10.9773 ± 0.0003 Å
• b: 18.0879 ± 0.0005 Å
• c: 16.4184 ± 0.0005 Å
• α: 90°
• β: 101.782 ± 0.0011°
• γ: 90°
• Cell volume: 3191.29 ± 0.16 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1551
• Weighted residual factors for all reflections included in the refinement: 0.1596
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No