Information card for entry 7710519

Structure parameters

• Formula: C26 H41 F3 Ge N2 O3 S Si2
• Calculated formula: C26 H41 F3 Ge N2 O3 S Si2
• Title of publication: Covalent triflates as synthons for silolyl- and germolyl cations
• Authors of publication: Wohltmann, Wiebke Marie; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 9.5398 ± 0.0005 Å
• b: 15.269 ± 0.0008 Å
• c: 22.8374 ± 0.0012 Å
• α: 85.5562 ± 0.0019°
• β: 89.91 ± 0.002°
• γ: 75.0746 ± 0.0018°
• Cell volume: 3204.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0749
• Weighted residual factors for all reflections included in the refinement: 0.0789
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No