Information card for entry 7710520

Structure parameters

• Formula: C36 H45 F3 N2 O3 S Si3
• Calculated formula: C36 H45 F3 N2 O3 S Si3
• Title of publication: Covalent triflates as synthons for silolyl- and germolyl cations
• Authors of publication: Wohltmann, Wiebke Marie; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 23.7374 ± 0.0019 Å
• b: 10.6333 ± 0.0008 Å
• c: 32.035 ± 0.003 Å
• α: 90°
• β: 111.229 ± 0.003°
• γ: 90°
• Cell volume: 7537.2 ± 1.1 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.1087
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No