Information card for entry 7710910

Structure parameters

• Formula: C69.75 H65.5 Cl3.5 I N2 O6 P4 Re
• Calculated formula: C68 H62 I0.999933 N2 O6 P4 Re
• Title of publication: Synthesis and anti-microbial activity of a new series of bis(diphosphine) rhenium(v) dioxo complexes
• Authors of publication: Cooper, Saul M.; Siakalli, Christina; White, Andrew J. P.; Frei, Angelo; Miller, Philip W.; Long, Nicholas J.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 29.5291 ± 0.0007 Å
• b: 29.5291 ± 0.0007 Å
• c: 24.5448 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 18534.9 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1396
• Weighted residual factors for all reflections included in the refinement: 0.151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No