Information card for entry 7710911

Structure parameters

• Formula: C66 H84 Cl N2 O8 P6 Re
• Calculated formula: C54 H52 N2 O8 P6 Re
• Title of publication: Synthesis and anti-microbial activity of a new series of bis(diphosphine) rhenium(v) dioxo complexes
• Authors of publication: Cooper, Saul M.; Siakalli, Christina; White, Andrew J. P.; Frei, Angelo; Miller, Philip W.; Long, Nicholas J.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.971 ± 0.0003 Å
• b: 14.1823 ± 0.0003 Å
• c: 18.7894 ± 0.0003 Å
• α: 91.9605 ± 0.0016°
• β: 101.288 ± 0.0016°
• γ: 114.163 ± 0.0019°
• Cell volume: 3067.27 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0505
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0717
• Weighted residual factors for all reflections included in the refinement: 0.0761
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No