Information card for entry 7711281

Structure parameters

• Formula: C36 H56 Na2 O2 Pb Si2
• Calculated formula: C36 H56 Na2 O2 Pb Si2
• Title of publication: Expanding the Series of Alkali Metal Plumbolyl Complexes to Na and K
• Authors of publication: Diaz-Rodriguez, Roberto; Kitos, Alexandros; Murugesu, Muralee
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 29.422 ± 0.002 Å
• b: 10.6642 ± 0.0009 Å
• c: 29.458 ± 0.002 Å
• α: 90°
• β: 111.437 ± 0.008°
• γ: 90°
• Cell volume: 8603.4 ± 1.2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.1218
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1112
• Weighted residual factors for all reflections included in the refinement: 0.1246
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No