Information card for entry 7711282

Structure parameters

• Formula: C36 H56 K2 O2 Pb Si2
• Calculated formula: C36 H56 K2 O2 Pb Si2
• Title of publication: Expanding the Series of Alkali Metal Plumbolyl Complexes to Na and K
• Authors of publication: Diaz-Rodriguez, Roberto; Kitos, Alexandros; Murugesu, Muralee
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 13.9365 ± 0.0003 Å
• b: 19.0723 ± 0.0003 Å
• c: 15.354 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4081.11 ± 0.13 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n 21 a
• Hall space group symbol: P -2ac -2n
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0207
• Weighted residual factors for significantly intense reflections: 0.0387
• Weighted residual factors for all reflections included in the refinement: 0.0434
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No