Information card for entry 7711283

Structure parameters

• Formula: C72 H120 K4 O8 Pb2 Si4
• Calculated formula: C72 H120 K4 O8 Pb2 Si4
• Title of publication: Expanding the Series of Alkali Metal Plumbolyl Complexes to Na and K
• Authors of publication: Diaz-Rodriguez, Roberto; Kitos, Alexandros; Murugesu, Muralee
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 13.9985 ± 0.0005 Å
• b: 14.6914 ± 0.0005 Å
• c: 20.5549 ± 0.0007 Å
• α: 90°
• β: 91.382 ± 0.002°
• γ: 90°
• Cell volume: 4226 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.0377
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0651
• Weighted residual factors for all reflections included in the refinement: 0.067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No