Information card for entry 7711770

Structure parameters

• Formula: C48 H54 Cl4 N4 W
• Calculated formula: C48 H54 Cl4 N4 W
• Title of publication: N Heterocyclic Carbene and Cyclic (Alkyl)(amino)carbene Complexes of Molybdenum(IV) and Tungsten(IV)
• Authors of publication: Luz, Christian; Glok, Eduard; Horrer, Günther; Radius, Udo
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.5166 ± 0.0001 Å
• b: 12.6137 ± 0.0001 Å
• c: 15.2964 ± 0.0001 Å
• α: 76.148 ± 0.001°
• β: 81.794 ± 0.001°
• γ: 75.425 ± 0.001°
• Cell volume: 2260.55 ± 0.03 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0232
• Residual factor for significantly intense reflections: 0.0224
• Weighted residual factors for significantly intense reflections: 0.0454
• Weighted residual factors for all reflections included in the refinement: 0.0457
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No